In this paper, we study the effect of using magnetorheological polydimethylsiloxane (MR-PDMS) spheres as micro optical resonators. Recently, optical sensors based on whispering gallery mode (WGM) have drawn much attention due to the high optical quality factors they can exhibit with several applications in a variety of fields. The modes of such resonators are highly affected by changes in morphology of the cavity (for instance: shape, size or refractive index) caused by a change in the physical input we are aiming to measure. In the presence of a magnetic field, the embedded particles become polarized, exerting forces upon one another because of dipolar interactions. In our case, these forces lead to changes in the morphology of the resonator through mechanical deformation of the size, which in turn causes WGM shifts. Experiments were conducted on earthworms for the similarity of the nerve impulses flowing which mimic those of human body specifically the brain and ultra-small magnetic fields can then be detected. Moreover, the coupling of a MR cantilever beam to the optical resonator leads to additional induced forces for the same magnetic field input and thus increasing the resolution by 3 orders of magnitude. Results indicate that the proposed sensor can be used for magnetic field detection with high quality factor and resolution.
In this paper, we develop dielectric micro-optical sensors based on whispering gallery mode phenomenon (WGM) for monitoring and treating of drinking water environments through two phases. Some sort of chemical impurities could be toxic and carcinogenic to humans and animals. The biogeochemical reactions are governing the chance and the movement of these impurities in the drinking water environment. Based on that, the first phase in this paper will focus to measure and quantify the concentration of these impurities in the water medium. While the second phase will exploit the use of the light based on the same phenomena (WGM) to create water treatment and purification using a nano charged dielectric polymeric beads. In the current paper, a high-resolution micro-optical sensor concept is used to detect these chemical impurities. The sensing element is a silica microsphere acts as an optical resonator. The proposed technique aims to provide preliminary results demonstrating the practical success of these sensors for effective monitoring of chemical impurities concentrations and contaminants which can cause serious kidney damage and possibly death. The second phase is basically depend on the optogenetic approach which is a biological technique that involves the use of light to control cells in living tissue, typically neurons that have been genetically modified to express light-sensitive ion channels. In this approach, the beads will be coated with a photosensitive protein called channelrhodopsin. This protein is a subfamily of retinylidene proteins (rhodopsins) that function as light-gated ion channels. They serve as sensory photoreceptors in unicellular green algae, controlling phototoxic: movement in response to light. The nano coated beads then poled for +4hrs under 1MV/m. When these nano charged beads mixed with water that have high turbidity, the beads starts to attract the colloids in that water. Since, the beads are coated with a photosensitive protein so by using a specific wavelength of the light we can control the motion of the spheres inside the water. Using a pulse width modulation (PWM) algorithm to control the speed of switching on/off the light; so it becomes easy to control the nano beads. The higher duty cycles for the PWM the charged beads makes the colloids aggregate and come together in a very short time (< 5 min) compared to the typical flocculation approaches that needs (~55min). This approach is called an optical flocculation technique and it shows one order of magnitude enhancement in the flocculation time. Results indicate that the WGM based-sensors are sensitive enough to refractive index changes in the case of liquid media (water). Experiments were carried out to validate the analysis and to provide an assessment of this sensor concept. Also, Preliminary experiments were carried out to provide an assessment of this concept using more than one duty cycle to control the speed of the beads. Results shows that we can purify the drinking water in time less than 3 minutes under 80% duty cycle using this approach.
The purpose of this paper is to identify fabrication methods for creating hollow optical whispering gallery modes (WGM) micro-resonators. These resonators are typically made from high optical polymeric materials like polydimethylsiloxane (PDMS) in solid shape which make it work as optical sensors once the round trip of the light is equal multiple integer of the wavelength that we used. The solid WGM resonators proved that it could reach a very high level of sensitivity for a certain input like (electric field, magnetic field and angular velocity,…etc.) but with a low bandwidth; because it behaved as an over damped system. On the other side, theoretically the hollow resonators can get the same level of sensitivity for the same input with an ultra-high bandwidth in kilo Hertz. A lot of sensing applications could be enhanced just using such a proposed sensor. Experimentally, we may consider the hollow resonators as simple harmonic oscillators. Accordingly, two parameters could be adjusted; the stiffness and the mass of the resonator. Since altering the stiffness coefficient requires us to change the material properties of the polymer we use and since there is a lot of constrains on the polymer material that avoid us to deal with it, based on that; changing the mass of the resonator is the only way for increasing its bandwidth. In conclusion, decreasing the mass of the sensor, making it hollow, can significantly affect its mechanical natural frequency leading to increase its bandwidth. Our challenge now is to fabricate these hollow resonators, since its typical size should range between couple of hundreds of micro-meters with fixed wall-thickness to let the optical resonance to occur. Different methods are being tested in this paper and currently we are finding more reliable ways to do it successfully. The first method will be by coating the hollow polymethylmethacrylate (PMMA) sphere with mechanically controlled syringe then a layer of PDMS base would be used as an outer layer which support the optical light to propagate through the resonator. The second method is to use the same hollow sphere but this time with the UV curable PDMS outer layer. The last method when using the microfluidic channels to create the hollow channels to create resonators using the gravitational force and its surface tension. All of these methods to produce these promising micro-optical hollow resonators will be shown with experimental analysis.
In the present work, we are demonstrating the capability of making polydimethylsiloxane (PDMS) microsphere sensors, which take advantage of an optical phenomenon called whispering gallery modes (WGM), a resonance condition happened when the optical path length of a laser in a polymeric microsphere is equal to an integer number of wavelengths, to make extraordinary electric field sensors capable of detecting electric fields. These sensors work by measuring the wavelength at which interference due to WGM occurs and then detecting when this value changes due to a change in the morphology of the spheres. This is possible since PDMS microspheres can be made to physically react to external electric fields. This physical reaction is called the electrostriction effect and governed by Navier’s equation for linear elasticity for steady state case. In this paper, an experiment will be conducted to find the angular orientation effects of the electric field on WGM optical sensors. In this experiment, the electric field is supplied by means of brass plates. These plates are mounted on a servo motor to provide the orientation angle of the applied electric field. The microsphere is placed between the plates. Prior to the experiment, the spheres are subjected to a high strength polling electric field of 1 MV/m. Initial results suggests that the sensitivity of the sphere has a dependence on the angular orientation of the sphere in the sensitizing polling electric field with respect to the orientation in the test electric field. This work we will show a definite relationship between the angular orientation in the sensitizing polling electric field and the response in the test electric field in order to maximize sensitivity. This has direct implications on eventual applications, since the orientation of a future sensor package will directly impact the sensitivity and performance of such a sensor used in the neurophotonics applications.
In this paper, an opto-mechanical frequency analyzer is designed using micro-optical dielectric resonators based on whispering gallery modes (WGM). Such an optical resonance phenomenon commonly referred to WGM, was excited by evanescently coupling light from a tunable laser diode using a tapered single-mode optical fiber. The proposed design is made from a canonical tube with array of dielectric beams placed inside which made from polydimethylsiloxane (PDMS) with different geometries. Once a sounds source connected from one end of the tube, the standing wave will perturb these polymeric beams. Then, spherical optical polymeric resonators mechanically coupled with the dielectric beams where placed at different locations to measure the acoustic radiation force. High resolution measurements will be achieved due to the high quality factor (Q-factor) of the resonator that can exhibit. Since, the canonical tube will has different resonant frequency at each certain location. The standing wave will perturb the WGM of the sensing element causing a shift in its transmission spectrum. Cross-correlation technique would be used to calculate that shift which called (WGM shifts). An analysis and calibrations are carried out along with preliminary designs and experiments. Results proved that the proposed technique could be used as a very high resolution frequency analyzer with practical success for bio-medical applications. Such a device could be used to split the sound into their component frequency exactly as an optical prism. This was done by creating a sensor that has the same design as the cochlea (inner ear) and placing optical sensors at different locations along the optical-cochlea to be able to detect different frequencies at the same time with high accuracy.
In this paper, novel techniques using ultra-sensitive chemical optical sensor based on whispering gallery modes (WGM) are proposed through two different configurations. The first one will use a composite micro-sphere, when the solvent interacts with the polymeric optical sensors through diffusion the sphere start to swallow that solvent. In turn, that leads to change the morphology and mechanical properties of the polymeric spheres. Also, these changes could be measured by tracking the WGM shifts. Several experiments were carried out to study the solvent induced WGM shift using microsphere immersed in a solvent atmosphere. It can be potentially used for sensing the trace organic solvents like ethanol and methanol. The second configuration will use a composite beam nitrocellulose composite (NC) structure that acts as a sensing element. In this configuration, a beam is anchored to a substrate in one end, and the other end is compressing the polymeric sphere causing a shift in its WGM. When a chemical molecule is attached to the beam, the resonant frequency of the cantilever will be changed for a certain amount. By sensing this certain resonant frequency change, the existence of a single chemical molecule can be detected. A preliminary experimental model is developed to describe the vibration of the beam structure. The resonant frequency change of the cantilever due to attached mass is examined imperially using acetone as an example. Breath diagnosis can use this configuration in diabetic’s diagnosis. Since, solvent like acetone concentration in human breath leads to a quick, convenient, accurate and painless breath diagnosis of diabetics. These micro-optical sensors have been examined using preliminary experiments to fully investigate its response. The proposed chemical sensor can achieve extremely high sensitivity in molecular level.
In this paper, we present a new fabrication method for the whispering gallery mode (WGM) micro-sphere based electric field sensor that which allows for longer time periods of sensitivity. Recently, a WGM-based photonic electric field sensor was proposed using a coupled dielectric microsphere-beam. The external electric field imposes an electrtrostriction force on the dielectric beam, deflecting it. The beam, in turn compresses the sphere causing a shift in its WGM. As part of the fabrication process, the PDMS micro-beams and the spheres are curied at high-temperature (100oC) and subsequently poled by exposing to strong external electric field (~8 MV/m) for two hours. The poling process allows for the deposition of surface charges thereby increasing the electrostriction effect. This methodology is called curing-then-poling (CTP). Although the sensors do become sufficiently sensitive to electric field, they start de-poling after a short period (within ~ 10 minutes) after poling, hence losing sensitivity. In an attempt to mitigate this problem and to lock the polarization for a longer period, we use an alternate methodology whereby the beam is poled and cured simultaneously (curing-while-poling or CWP). The new fabrication method allows for the retention of polarization (and hence, sensitivity to electric field) longer (~ 1500 minutes). An analysis is carried out along with preliminary experiments. Results show that electric fields as small as ~ 100 V/m can be detected with a 300 μm diameter sphere sensor a day after poling.
In this paper, a high-resolution bio-optical sensor is developed for brain activity measurement. The aim is to develop an optical sensor with enough sensitivity to detect small electric field perturbations caused by neuronal action potential. The sensing element is a polymeric dielectric micro-resonator fabricated in a spherical shape with a few hundred microns in diameter. They are made of optical quality polymers that are soft which make them mechanically compatible with tissue. The sensors are attached to or embedded in optical fibers which serve as input/output conduits for the sensors. Hundreds or even thousands of spheres can be attached to a single fiber to detect and transmit signals at different locations. The high quality factor for the optical resonator makes it significantly used in such bio-medical applications. The sensing phenomenon is based on whispering gallery modes (WGM) shifts of the optical sensor. To mimic the brain signals, the spherical resonator is immersed in a homogeneous electrical field that is created by applying potential difference across two metallic plates. One of the plates has a variable voltage while the volt on the other plate kept fixed. Any small perturbations of the potential difference (voltage) lead to change in the electric field intensity. In turn the sensor morphology will be affected due to the change in the electrostriction force acting on it causing change in its WGM. By tracking these WGM shift on the transmission spectrum, the induced potential difference (voltage change) could be measured. Results of a mathematical model simulation agree well with the preliminary experiments. Also, the results show that the brain activity could be measured using this principle.
A computational model for the whispering gallery modes inside a microsphere resonator is presented. In the archetypical microsphere resonator sensor, a tunable laser light beam is injected into an optical fiber and coupled with the resonator’s cavity. The resonant optical coupling is achieved by bringing the fiber in the vicinity of the cavity’s evanescent field. The transmission spectrum is then observed to detect the WGM shifts. In this paper, two-dimensional models of a single laser source put near the equator of a microsphere are simulated using COMSOL Multi-physics 5.1 electromagnetic waves, beam envelopes library. Afterwards, a three-dimensional model of two laser sources put near the horizontal and vertical equators of a microsphere is computed. The transmission spectrum of both simulations was taken and cross correlation was performed on them. Results show a big similarity between both simulations and could bring a breakthrough in the area of optical sensors.
A novel approach for tracking of whispering gallery modes (WGM) in real-time for dielectric cavities used in sensing application is presented in this paper. Real-time tracking for the shifts of the WGM can be used to measure the physical quantity of interest precisely, under high repetition rates. The tracking algorithm is based on cross-correlation signal processing technique which has been proved to be accurate in WGM shifts detection. In order to achieve portability, the aforementioned real-time algorithm is implemented using a single-board re-configurable input-output hardware. The hardware platform used combines a real-time processor and a field programmable gate array (FPGA), it also allows for data exchange between them. The tracking algorithm’s accuracy and real-time behavior is verified by preforming simulations based on experiments conducted on the dielectric cavity, where the cavity is used as a force sensor measuring mechanical compression. The light from a laser diode is tuned with rates up to 10 kHz and then tangentially coupled into the cavity to excite the WGM. Results show that shifts of the WGM are tracked by the algorithm providing real-time force readings.
This paper studies the effect of the electrostriction force on the single optical dielectric core coated with multi-layers based on whispering gallery mode (WGM). The sensing element is a dielectric core made of polymeric material coated with multi-layers having different dielectric and mechanical properties. The external electric field deforming the sensing element causing shifts in its WGM spectrum. The multi-layer structures will enhance the body and the pressure forces acting on the core of the sensing element. Due to the gradient on the dielectric permittivity; pressure forces at the interface between every two layers will be created. Also, the gradient on Young’s modulus will affect the overall stiffness of the optical sensor. In turn the sensitivity of the optical sensor to the electric field will be increased when the materials of each layer selected properly. A mathematical model is used to test the effect for that multi-layer structures. Two layering techniques are considered to increase the sensor’s sensitivity; (i) Pressure force enhancement technique; and (ii) Young’s modulus reduction technique. In the first technique, Young's modulus is kept constant for all layers, while the dielectric permittivity is varying. In this technique the results will be affected by the value dielectric permittivity of the outer medium surrounding the cavity. If the medium’s dielectric permittivity is greater than that of the cavity, then the ascending ordered layers of the cavity will yield the highest sensitivity (the core will have the smallest dielectric permittivity) to the applied electric field and vice versa. In the second technique, Young's modulus is varying along the layers, while the dielectric permittivity has a certain constant value per layer. On the other hand, the descending order will enhance the sensitivity in the second technique. Overall, results show the multi-layer cavity based on these techniques will enhance the sensitivity compared to the typical polymeric optical sensor.
Spinning spherical resonators in the torsional vibrational applications could cause a shift in its whispering gallery mode (WGM). The centripetal force acting on the spinning micro sphere resonator will leads to these WGM shifts. An analysis and experiment were carried out in this paper to investigate and demonstrate this effect using different polymeric resonators. In this experiment, centripetal force exerted by the DC-Motor on the sphere induces an elastic deformation of the resonator. This in turn induces a shift in the whispering gallery modes of the sphere resonator. Materials used for the sphere are polydimethylsiloxane (PDMS 60:1 where 60 parts base silicon elastomer to 1 part polymer curing agent by volume) with shear modulus (G≈1kPa), (PDMS 10:1) with shear modulus (G≈300kPa), polymethylmethacrylate (PMMA, G≈2.6×109GPa) and silica (G≈3×1010 GPa). The sphere size was kept constant with 1mm in diameter for all above materials. The optical modes of the sphere exit using a tapered single mode optical fiber that is coupled to a distributed feedback laser. The transmission spectrum through the fiber is monitored to detect WGM shifts. The results showed the resonators with smaller shear modulus G experience larger WGM shift due to the larger mechanical deformation induced by the applied external centripetal force. Also, the results show that angular velocity sensors used in the torsional vibrational applications could be designed using this principle.
In this paper, we demonstrate the use of whispering gallery mode (WGM) resonators for high-speed transient sensing. In the typical WGM sensor, the micro-resonator modes are interrogated by coupling light from a tunable laser through a single mode optical fiber. The laser is tuned over a narrow range by thermo-optic effect, and mode shifts in the transmission spectrum through the fiber are observed. For high-speed applications, thermal inertia of the optical system impedes the proper tuning of the laser, limiting the WGM sensor applications to slow varying phenomena. In order to use the sensors for high-speed transient applications, we tune the DFB laser using a harmonic rather than a ramp waveform and calibrate the laser response at various input frequencies and amplitudes using a Fabry-Perot interferometer. WGM shifts are tracked using a fast cross-correlation algorithm on the transmission spectra. We demonstrate dynamic force measurements up to 10 kHz using this approach. We also present a simple lumped-heat capacity thermal model to predict the laser response.
In this paper we present a beam-coupled micro-optical sensor for electric field detection. The main components of the sensor are a microsphere optical resonator and a dielectric micro-beam. The dielectric beam is coupled with the microsphere using two different approaches. In the first approach the beam compresses the sphere causing a shift in its whispering gallery mode (WGM). In the second approach the fine tipped beam perturbs the evanescent field of the sphere thereby causing a shift its WGM. In this approach, electrostriction force exerted by the electric field on the beam induces a change in the gap between sphere and beam perturbing the evanescent field of the sphere. This in turn induces a shift in the whispering gallery modes of the sphere resonator. The material for both the sphere and the beam in the first approach is polydimethylsiloxane (PDMS). The resonator and the beam are made of silica in the second approach. Different beam and sphere sizes are studied to optimize the proposed sensor’s electric field resolution. The optical modes of the sphere are exited using a tapered single mode optical fiber that is coupled to a distributed feedback laser. The transmission spectrum through the fiber is monitored to detect WGM shifts.
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